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Contaminants In general, acid copper tolerates both organic and metallic contaminants. Organic residues may come from cleaners, resists, and certain sulfur compounds. Dye systems usually are more resistant than dye-free systems with respect to certain cleaner constituents.

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Now that your creative juices are owing, it s time to focus on why you re speaking. Keep these three questions in mind during the entire preparation process: 1. What do I want my audience to know 2. What do I want my audience to do 3. What do I want my audience to feel You may doubt that the way your listeners feel really matters to your presentation, but remember that humans are emotional beings, so every decision we make has an emotional component. If you can create a feeling of anxiety around a problem and then turn that feeling to relief and anticipation as a result of your solution, you re on your way to having the audience hooked. The mood generated by your presentation has a strong effect on you and your listeners. Next, create a purpose or goal statement. The statement should be speci c and geared toward what the audience will gain from listening. Here are some examples: At the end of my presentation . . . My audience will understand the value of my product and agree to include it in their next catalog. My audience will understand and accept the reasons why this project is necessary for their organization to undertake as soon as possible. The audience will learn at least three value-added ideas they can incorporate into their next sales meeting. As you work on the presentation, keep this goal statement in mind to maintain your focus. Like a map, it shows you how to keep heading in the right direction.

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Applying the appropriate transformation matrix to the Ricci rotation coef cients, one nds that r is (a) r sin2 (b) r sin2 (c) cot r (d) r12 Consider the Rindler metric, ds 2 = u 2 dv 2 du 2 . One nds that nonzero Ricci rotation coef cients are 1 (a) v v v = u u v = u (b) The space is at, so all the Ricci rotation coef cients vanish. (c) u v v = v u v = u12 1 v u (d) uv = u vv =

Metals should be kept at these maximums: chromium, 25 ppm; tin, 300 ppm; antimony, 25 ppm. Nickel, lead, and arsenic may also cause roughness and other problems.

Copper sulfate is the source of metal. Low copper will cause deposit burning; high copper will cause roughness and decreased hole-to-surface thickness ratios or throwing power. Sulfuric acid increases the solution conductivity, allowing the use of high currents at low voltages. However, an excess of sulfuric acid lowers the plating rate, whereas low acid reduces holeto-surface ratio (throwing power). Chloride ion (Cl ) should be controlled at 60 to 80 ppm. Below 30 ppm, deposits will be dull, striated, coarse, and step-plated. Above 120 ppm, deposits will be coarse-grained and dull. The anodes will become polarized, causing plating to stop. Excess chloride is reduced by bath dilution or by dragout. Additive components analysis and control are critical for consistent product quality. The primary analytical tool is CVS, and the Hull cell continues to be a useful complementary tool. Excessive or insufficient additive will cause deposit burning and corner cracking. This condition can be judged by metallographic cross-sectioning and etching. Optimum-quality plated metal is fine-grained and equiaxed (nondirectional) and shows no laminations or columnar patterns. Concerning water quality, the use of DI water and contamination-free materials such as low chloride and iron will give added control and improved deposit quality.

29.6.3.2 Temperature. Optimum throwing power and surface-to-hole ratios are obtained by operating at room temperature (i.e., 70 to 80 F). Lower temperatures cause brittleness, burning, and thin plating. Higher temperatures cause haze in low-current-density areas and reduced throwing power. Cooling coils may be necessary during a hot summer or under heavy operation. 29.6.3.3 Deposition Rate. A thickness of 0.001 in. (1.0 mil) of copper deposits in 54 min. at 20 A/ft2, in 21 min. at 50 A/ft2. 29.6.3.4 Hull Cell. Operation at 2 A will show the presence of organic contamination, chloride concentration, and overall bath condition. However, an optimum Hull cell panel is only a small indication that the bath is in good operating condition, since test results are not always related to production problems. More reliable results are obtained by adjusting the bath before Hull cell testing. See Sec. 29.12.4 for procedures on Hull cell.

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