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Cross-Sectioning Results Troubleshooting Sectioning with etching provides information on the plated copper that explains PTH quality in terms of processing factors. Besides showing the overall quality, cross-sectioning gives information on thickness and on possible problems, such as drilling, cracking, blowholes, and multilayer smear. Copper deposits with columnar or laminar patterns indicate inferior copper properties. Cross sections of optimum copper deposits are fine-grained and equiaxed (structureless) upon etching.

Inferior Copper Deposits These may be caused by any of the following:

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Either low or excess additives Chloride out of range (i.e., too high or too low) Organic, metal, or sulfur (thiourea) contamination Excess DC rectifier ripple (greater than 10 percent) Low copper content with bath out of balance Roughness in drilling, voids in electroless steps, or other problems introduced in earlier processing

Resistance to cracking is tested by the following:

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Solder reflow Wave soldering and cross-sectioning are acceptable alternatives. Elongation Two mil copper foil should exceed 10 percent elongation. Acid copper elongation should range between 10 and 25 percent. Frequent testing gives more meaningful results. Float solder test This test includes prebaking and flux, using a 5 to 20 sec. float in a solder pot (60:40) at 550 F, followed by cross-sectioning for evaluation. Copper foil bulge test This test measures tensile strength by puncturing copper at high pressure. DC ripple High values of rectifier ripple (8 to 12 percent) may cause inferior copper deposits and poor distribution of thickness.

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29.6.5.2 Visual Appearance. When plated, copper has a semibright appearance at all current densities. Unevenness, hazy or dull deposits, cracking, haloing around the PTH, and lowcurrent-density areas indicate organic contamination. Carbon treatment is required if these conditions persist. Burned, dull deposits at high-current densities indicate low additive content, contamination, solution imbalance, or low bath temperatures. If dull, coarse deposits result at low-current densities, the chloride ion is not in balance. When chloride is high or bath temperature too low, anodes may become heavily coated and polarized (the current drops). Decreased throwing power (surface-to-hole ratio), reduced bath conductivity, or poor-quality plating may also indicate contamination and are corrected as follows:

Maintaining solution balance and chloride content at 60 to 80 ppm Circulating solution through filter continuously, passing through a carbon canister periodically, or by batch carbon treatment Analyzing organic additives by CVS or Hull cell Checking metal contaminations every three months Keeping the temperature between 70 and 85 F Checking anodes daily and replacing bags and filters (rinsed in hot water) every three to four weeks

Why me You might be asking yourself why you are the one who is expected to stand in front of an audience Most commonly, a speaker is selected because he or she ts into at least one of the following categories: A subject matter expert (SME), that is, someone who knows a subject in depth Television news shows will often interview a doctor about a health-related issue, an attorney about a legal case, or a retired general about a military initiative Hint: Just because someone is an SME, don t assume that person is the most skilled communicator! The most senior person on the team or within the organization The person with seniority is often selected to speak because that person has in uence, credibility, or the perspective to offer the big picture The senior person will often give an overview and will be the rst of several speakers.

29.6.5.3 Problems. Table 29.5 lists problems that appear after copper plating. Two groups are listed, with the first group readily correlated to the copper-plating process. Thin, rough copper plating in the PTH may also be exhibited by outgassing and blowholes during wave soldering. Figures 29.16 through 29.25 illustrate some of these effects.

TABLE 29.5 Printed Wiring Board Copper-Plating Defects Defect in copper process Corner cracking Nodules Thickness distribution Dullness Uneven thickness in PTH Pitting Columnar deposits Step plating, whiskers Defect, overall manufacturing process Voids etching Inner layer smear Roughness Hole-wall pullaway Copper-copper peeling Soldering blowholes Cause Excess additive, organic contamination in solution Particulate matter in solution; also drilling, deburring residues See Sec. 29.5.2 Off-balance solution, organic contamination Organic sulfur (thiourea) contamination Additive malfunction, defective electroless, or preplate preparation Low additive, rectifier malfunction Excess or defective additive Cause Malfunction of electroless copper steps, also preplate cleaner Drilling or malfunction in smear removal Drilling or drilling residues Malfunction of smear removal or electroless copper steps Surface residues from electroless and/or image transfer Drilling roughness, voids, and thin plating

FIGURE 29.20 PTH vertical cross section illustrating rough, nodular copper plating due to drilling roughness. Nail-heading is also shown.

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