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29.9.1.1 Process Controls pH With normal operation, pH increases. To lower pH, use sulfamic acid (not sulfuric acid). A decrease in pH signals a problem; anodes should be checked. Temperature The preferred temperature is 125 F. Low temperature causes stress and highcurrent-density (CD) burning. Higher temperatures increase softness of nickel deposit. Agitation Solution circulation between panels is done by filter pump and/or cathode rod agitation. Filtration This is done continuously through 5 to 10 mm polypro filter, which is changed weekly. Deposition rate For 0.5 mil, plate 25 to 30 min. at 25 A/ft2. For 0.2 to 0.3 mil, plate 15 min. 2 at 25 A/ft . Contaminations These include three groups of contaminants: Metals The following are the maximum allowable metal content by atomic absorption: iron, 250 ppm; copper, 10 ppm; chromium, 20 ppm; aluminum, 60 ppm; lead, 3 ppm; zinc, 10 ppm; tin, 10 ppm; and calcium, 0 ppm. These metal contaminants lower the deposition rates and cause nonuniform plating. Cooper and lead cause dark, brittle deposits at low CD. Dummy-plate at 3 to 5 A/ft2. Iron, tin, lead, and calcium cause deposit roughness and stress. Organics These cause pitting, brittleness, step plating, and lesser ductility. Sulfates These cause solution breakdown and should not be added. Carbon treatment Circulate through a carbon canister for 4 hours (more than one canister may be required) or batch-treat to remove organics.The basic six steps to batch-carbon-treat are as follows: 1. 2. 3. 4. 5. 6. Heat to 140 F. Transfer to the treatment tank. Do not adjust pH. Add 3 to 5 lb. carbon per 100 gal of solution. Premix outdoors. Stir 4 hours at temperature. Let the solution settle 1 to 2 hour. Filter the solution back to cleaned tank.

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29.9.1.2 Common Problems. Pitting, stress (cracking), and burned deposits are common problems:

Pitting This is caused by low antipit, poor agitation or circulation, boric acid imbalance, or the presence of organics. In testing for antipit, the solution should hold bubble for 5 sec. in a 3 in. wire ring and for less than 5 sec. in a 5 in. ring. In the case of severe pitting, cool to room temperature, add 1 pt/200 gal hydrogen peroxide (35 percent), bubble air, and reheat to 140 F. Carbon-treat as described in Sec. 29.9.1.1. Adjust pH before restarting. Stress This refers to the cause of deposit cracking. Although low nickel chloride causes poor anode corrosion (a rapid decrease in nickel content), high chloride causes excess stress. To prevent this, maintain pH, current density, and boric acid for control below 10 kpsi. Burns A low level of nickel sulfamate causes high-current-density burns. Common treatment includes the following:

Hull cell Plate at 2 A for 10 min. with gentle agitation. This test is useful for bath condition and contaminants.

Visual observation The plated metal has a matte, dull finish. Burned deposits are caused by low temperature, high-current density, bath imbalance, and poor agitation. Rough deposits are due to poor filtration, pH out of spec, contamination, or high-current density.

Pitting is due to low antipit, poor agitation, bath imbalance, or organic contamination. Low plating rates are due to low pH, low-current density, or impurities. Gassing at the cathode is a sign of low plating rates.

Nickel Sulfate This is typically plated with an automatic edge connector (tip) plating machine. Table 29.9 gives the operating conditions that apply to these systems. For additional instruction, follow the details in Sec. 29.9.1.

TABLE 29.9 Nickel Sulfate: Operation and Control Operating conditions: pH Nickel Nickel chloride Boric acid Stress reducer Antipit Temperature Cathode current density Current efficiency Anodes: Composition

1.5 4.5 15 17 oz./gal 2 4 oz./gal (with soluble anodes) 5 7 oz./gal As required As required 130 5 F 100 600 A/ft2 65% Nickel or platinized titanium

Nickel anodes are preferred in tip machines because the pH and the metal content remain stable. The pH will decrease rapidly when insoluble anodes are used. The pH should be maintained at 1.5 or higher with additions of nickel carbonate. Stress values are higher than in sulfamate baths, with values of about 20 kpsi.

Early printed circuit board technology used gold extensively. In addition to being an excellent resist for etching, gold has good electrical conductivity, tarnish resistance, and solderability after storage. Gold can produce contact surfaces with low electrical resistance. In spite of its continued advantages, the high cost of gold has restricted its major application to edge connectors (tips) and selected areas, with occasional plating on pads, holes, and traces (body gold). Both hard-alloy and soft, pure gold are currently used. Plating solutions are acid (pH 3.5 to 5.0) and neutral (pH 6 to 8.5). Both automatic plating machines for edge connectors and manual lines are in use.

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