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Direct Chlorination Cu2Cl2 + Cl2 2CuCl2 (346) As the traditional regeneration choice, the chlorine reaction is rapid, positive, and easily controlled Liquefied chlorine gas has been generally available, and standardized commercial addition systems have been available Recently, pressure on chlorine distribution and use due to safety and environmental regulations have made availability and implementation more expensive and difficult It is significant that the reaction simplicity indicates that all etched copper is converted directly to cupric chloride (combination of Eqs 343 and 346)Thus, there is no effect on water or acid balances from the etching reaction itself Hydrogen Peroxide Cu2Cl2 + 2H2O2 + 2HCl 2CuCl2 + 2H2O (347) This process is more complicated because both hydrogen peroxide and hydrochloric acid add water in the reaction process. excel ean 128 How to create GS1 - 128 Barcodes in Excel using the Code 128 Font ...
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Code 128 & GS1 - 128 Code for Excel . Create Code 128 and GS1 - 128 barcodes in your spreadsheets using our Excel macros along with our software and fonts . Since hydrogen peroxide is unsafe to store and handle in concentrations above 35 percent, there is considerable water added with both the oxidizer and the hydrochloric acid The result limits the copper-holding capacity of the etchant The addition is reasonably and simply controlled as a direct ratio of HCl, and peroxide is added to the bath to maintain the copper oxidation This formulation has been favored in Europe and to some extent in Asia Sodium Chlorate 3Cu2Cl2 + NaClO3 + 6HCl 6CuCl2 + NaCl + 3H2O (348) Sodium chlorate has become one of the most widely used formulations The oxidizer solutions can be mixed from powder and are also commercially supplied as 45 percent solutions The water balance must also be carefully controlled with this oxidizing plan, and the amount of sodium chloride in the working bath can be boosted by addition with the oxidizer. ean 128 excel macro Create Barcodes With (Or Without) Excel VBA
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EAN -13 and EAN -8 codes, which means European ... Download the Code128 and Code 39 barcode fonts . This can be a rate enhancer by supplying chloride ions needed by Eq (346), and since the chloride ion is separately added from the hydrochloric acid, the free acid can be maintained at very low levels (<01 normal).. Electrolytic (Cathode) (Anode) Cu+ + e Cu Cu+ Cu2+ + e (34.9) (34.10) excel ean 128 barcode GS1 - 128 barcode Excel macros from Azalea Software
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Code 128 & GS1 - 128 barcode Excel macros from Azalea Software. Free macros, free tech support and a 30 day money-back guarantee. Buy online, download ... Electrolytic systems of direct and membrane cell design have been employed. However, this technology is not a major factor in current manufacturing practice. 34.4.2.2 Properties and Control. Early cupric chloride formations had slow etch rates and low copper capacity and were limited to batch operation.15 21 Regenerated continuous operation using modified formulations has brought useful improvements. Etch rates as high as 55 s for 1 oz copper are obtained from cupric chloride sodium chloride HCl systems operated at 130 F with conventional spray-etching equipment. Copper capacities are maintained at 20 oz/ gal and above. However, more recently, higher copper contents and adjusted chemistries at 125 F typically etch at 75 to 90 s for 1 oz copper. 34.4.2.3 Continuous Etching and Regeneration. Systems in use include chlorination, sodium chlorate, hydrogen peroxide, and electrolysis. Chlorination. Direct chlorination has been the preferred technique for regeneration of cupric etchant because of its historically low cost, high rate, efficiency in recovery of copper, and pollution control. The cupric chloride sodium chloride system (Table 34.1, no. 3) is suitable. Figure 34.2 shows a generalized process.17 Chlorine, hydrochloric acid, and sodium chloride solutions are automatically fed into the system as required. Sensing devices include oxidation-reduction instruments (Cu oxidation state), density (Cu concentration), level sensors, 291 294 295 297 301 303 304 311 312 318 321 322 323 329 333 337 Chloride Additive Tank (HCl, NaCl) and thermostats Chlorination is reliable and controllable Other factors are safety and solution control Optical colorimetric sensors can be used to detect Cu(I) levels However, these cells are subject to fogging by organic contamination and crystalline buildup with the hazardous defect of continuing to add chemicals past the proper control points and liberating chlorine into the work area 1 Safety Use of chlorine gas requires adequate ventilation, tank and cylinder storage, leak-detection equipment, emergency protocols, personal protective equipment, operator training, and fire department approval and inspection of installations 2 Solution control An increase in pH will cause the copper colorimeter to give erroneous readings caused by turbidity in the solution Organic deposits can also foul controls Excess NaCl at 18 to 20 oz/gal copper causes coprecipitation of salts when the solution is cooled Solution filtration and etch tank cleanliness must be maintained. Replacement of electrodes, instruments, and metering devices should be scheduled regularly Chlorate Regeneration This method, currently widely supported, uses sodium chlorate, sodium chloride, and hydrochloric acid and is an alternate method similar to chlorination A control sequence similar to the one shown in Fig 342 may be used Sodium chlorate is available in commercial solutions of several strengths with some degree of formulated agents (usually sodium chloride) added to the mixture These solutions are added with hydrochloric acid either as a coordinated addition or in a special control logic sequence that allows very low free acid This control system uses a multiple sensor color or turbidimetric optical system The addition of one component (eg, oxidizer) to a flowing sample cell occurs when the primary cell senses are triggered A second cell allows this addition so long as there is a change from the first cell input. barcode ean 128 excel EAN 128 Barcode Generator for Microsoft Excel
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